Synthesis of yttria nanopowders by two precipitation methods and investigation of synthesis conditions

Mohammad Khajelakzay; Reza Shoja Razavi; Masoud Barekat; Mahdi Naderi; Mostafa Milani

doi:10.1111/ijac.12430

Synthesis of yttria nanopowders by two precipitation methods and investigation of synthesis conditions

Mohammad Khajelakzay, Reza Shoja Razavi, Masoud Barekat, Mahdi Naderi, Mostafa Milani

Research output: Journal Publication › Article › peer-review

21 Citations (Scopus)

Abstract

Yttrium oxide nanopowder was successfully synthesized by two precipitation methods, through which Y₂O₃ nanopowder was prepared by ammonium hydroxide and ammonium hydrogen carbonate as precipitants. Hydroxide and carbonate precursors of Y₂O₃ with approximate composition of Y(OH)₃ and Y₂(CO₃)₃, respectively, were synthesized using yttrium nitrate as the starting salt. XRD results show cubic yttrium oxide phase for annealed samples. SEM and TEM images show that samples are composed of agglomerated and nonagglomerated nanoparticles with different shapes and sizes. Optimal conditions for synthesis of nanoparticles were defined as 3-h aging time, ammonium hydrogen carbonate as precipitant, and calcination temperature of 1000°C.

Original language	English
Pages (from-to)	209-218
Number of pages	10
Journal	International Journal of Applied Ceramic Technology
Volume	13
Issue number	1
DOIs	https://doi.org/10.1111/ijac.12430
Publication status	Published - 1 Jan 2016
Externally published	Yes

ASJC Scopus subject areas

Ceramics and Composites
Condensed Matter Physics
Marketing
Materials Chemistry

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title = "Synthesis of yttria nanopowders by two precipitation methods and investigation of synthesis conditions",

abstract = "Yttrium oxide nanopowder was successfully synthesized by two precipitation methods, through which Y2O3 nanopowder was prepared by ammonium hydroxide and ammonium hydrogen carbonate as precipitants. Hydroxide and carbonate precursors of Y2O3 with approximate composition of Y(OH)3 and Y2(CO3)3, respectively, were synthesized using yttrium nitrate as the starting salt. XRD results show cubic yttrium oxide phase for annealed samples. SEM and TEM images show that samples are composed of agglomerated and nonagglomerated nanoparticles with different shapes and sizes. Optimal conditions for synthesis of nanoparticles were defined as 3-h aging time, ammonium hydrogen carbonate as precipitant, and calcination temperature of 1000°C.",

author = "Mohammad Khajelakzay and \{Shoja Razavi\}, Reza and Masoud Barekat and Mahdi Naderi and Mostafa Milani",

note = "Publisher Copyright: {\textcopyright} 2015 The American Ceramic Society.",

year = "2016",

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doi = "10.1111/ijac.12430",

language = "English",

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TY - JOUR

T1 - Synthesis of yttria nanopowders by two precipitation methods and investigation of synthesis conditions

AU - Khajelakzay, Mohammad

AU - Shoja Razavi, Reza

AU - Barekat, Masoud

AU - Naderi, Mahdi

AU - Milani, Mostafa

PY - 2016/1/1

Y1 - 2016/1/1

N2 - Yttrium oxide nanopowder was successfully synthesized by two precipitation methods, through which Y2O3 nanopowder was prepared by ammonium hydroxide and ammonium hydrogen carbonate as precipitants. Hydroxide and carbonate precursors of Y2O3 with approximate composition of Y(OH)3 and Y2(CO3)3, respectively, were synthesized using yttrium nitrate as the starting salt. XRD results show cubic yttrium oxide phase for annealed samples. SEM and TEM images show that samples are composed of agglomerated and nonagglomerated nanoparticles with different shapes and sizes. Optimal conditions for synthesis of nanoparticles were defined as 3-h aging time, ammonium hydrogen carbonate as precipitant, and calcination temperature of 1000°C.

AB - Yttrium oxide nanopowder was successfully synthesized by two precipitation methods, through which Y2O3 nanopowder was prepared by ammonium hydroxide and ammonium hydrogen carbonate as precipitants. Hydroxide and carbonate precursors of Y2O3 with approximate composition of Y(OH)3 and Y2(CO3)3, respectively, were synthesized using yttrium nitrate as the starting salt. XRD results show cubic yttrium oxide phase for annealed samples. SEM and TEM images show that samples are composed of agglomerated and nonagglomerated nanoparticles with different shapes and sizes. Optimal conditions for synthesis of nanoparticles were defined as 3-h aging time, ammonium hydrogen carbonate as precipitant, and calcination temperature of 1000°C.

UR - https://www.scopus.com/pages/publications/84954150316

U2 - 10.1111/ijac.12430

DO - 10.1111/ijac.12430

M3 - Article

AN - SCOPUS:84954150316

SN - 1546-542X

VL - 13

SP - 209

EP - 218

JO - International Journal of Applied Ceramic Technology

JF - International Journal of Applied Ceramic Technology

IS - 1

ER -

Synthesis of yttria nanopowders by two precipitation methods and investigation of synthesis conditions

Abstract

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