Synthesis, characterization and optical properties of Zr+4/La+3/Nd+3 tri-doped yttria nanopowder by sol-gel combustion method

Shima Shirinparvar; Reza Shoja Razavi; Fatemeh Davar; Mohammad Reza Loghman-Estarki; Morteza Hajizadeh-Oghaz; Saeid Ghorbani

doi:10.1016/j.ceramint.2016.03.054

Synthesis, characterization and optical properties of Zr⁺⁴/La⁺³/Nd⁺³ tri-doped yttria nanopowder by sol-gel combustion method

Shima Shirinparvar, Reza Shoja Razavi, Fatemeh Davar, Mohammad Reza Loghman-Estarki, Morteza Hajizadeh-Oghaz, Saeid Ghorbani

Research output: Journal Publication › Article › peer-review

22 Citations (Scopus)

Abstract

In this research, zirconium lanthanum and neodymium tri-doped yttria nanopowder was synthesized using the sol-gel combustion method. Citric acid (CA) and glycine (G) were used for the gel and fuel agent, respectively. The effect of CA:G:TM (TM=transition metal) mole ratios on the particle size and morphology of the product was evaluated. As-synthesized samples were characterized by X-ray diffraction (XRD), field-emission scanning electron microscope (FESEM), transmission electron microscope (TEM), energy dispersion spectrum (EDS), photoluminescence (PL) spectrum, Inductively coupled plasma (ICP), UV-visible (UV-vis spectroscopy), thermal gravimetric-differential thermal analysis (TG/DTA) and Fourier transform infrared (FTIR)analysis. The optimized sample synthesized with CA:G:TM mole ratio of (1.06:1.06:1) had the average particle size of 30-40 nm with a spherical morphology. Moreover, the optimized sample showed visible photoluminescence, at 400-800 nm.

Original language	English
Pages (from-to)	10551-10558
Number of pages	8
Journal	Ceramics International
Volume	42
Issue number	9
DOIs	https://doi.org/10.1016/j.ceramint.2016.03.054
Publication status	Published - 1 Jul 2016
Externally published	Yes

Keywords

Citric acid
Glycine
Sol-gel combustion
Zirconium lanthanum and neodymium tri-doped yttria nanopowder

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Ceramics and Composites
Process Chemistry and Technology
Surfaces, Coatings and Films
Materials Chemistry

Access to Document

10.1016/j.ceramint.2016.03.054

Cite this

@article{afdf82a470ba40d399766d27ffe26885,

title = "Synthesis, characterization and optical properties of Zr+4/La+3/Nd+3 tri-doped yttria nanopowder by sol-gel combustion method",

abstract = "In this research, zirconium lanthanum and neodymium tri-doped yttria nanopowder was synthesized using the sol-gel combustion method. Citric acid (CA) and glycine (G) were used for the gel and fuel agent, respectively. The effect of CA:G:TM (TM=transition metal) mole ratios on the particle size and morphology of the product was evaluated. As-synthesized samples were characterized by X-ray diffraction (XRD), field-emission scanning electron microscope (FESEM), transmission electron microscope (TEM), energy dispersion spectrum (EDS), photoluminescence (PL) spectrum, Inductively coupled plasma (ICP), UV-visible (UV-vis spectroscopy), thermal gravimetric-differential thermal analysis (TG/DTA) and Fourier transform infrared (FTIR)analysis. The optimized sample synthesized with CA:G:TM mole ratio of (1.06:1.06:1) had the average particle size of 30-40 nm with a spherical morphology. Moreover, the optimized sample showed visible photoluminescence, at 400-800 nm.",

keywords = "Citric acid, Glycine, Sol-gel combustion, Zirconium lanthanum and neodymium tri-doped yttria nanopowder",

author = "Shima Shirinparvar and Razavi, \{Reza Shoja\} and Fatemeh Davar and Loghman-Estarki, \{Mohammad Reza\} and Morteza Hajizadeh-Oghaz and Saeid Ghorbani",

note = "Publisher Copyright: {\textcopyright} 2016 Elsevier Ltd and Techna Group S.r.l.",

year = "2016",

month = jul,

day = "1",

doi = "10.1016/j.ceramint.2016.03.054",

language = "English",

volume = "42",

pages = "10551--10558",

journal = "Ceramics International",

issn = "0272-8842",

publisher = "Elsevier Ltd.",

number = "9",

}

TY - JOUR

T1 - Synthesis, characterization and optical properties of Zr+4/La+3/Nd+3 tri-doped yttria nanopowder by sol-gel combustion method

AU - Shirinparvar, Shima

AU - Razavi, Reza Shoja

AU - Davar, Fatemeh

AU - Loghman-Estarki, Mohammad Reza

AU - Hajizadeh-Oghaz, Morteza

AU - Ghorbani, Saeid

PY - 2016/7/1

Y1 - 2016/7/1

N2 - In this research, zirconium lanthanum and neodymium tri-doped yttria nanopowder was synthesized using the sol-gel combustion method. Citric acid (CA) and glycine (G) were used for the gel and fuel agent, respectively. The effect of CA:G:TM (TM=transition metal) mole ratios on the particle size and morphology of the product was evaluated. As-synthesized samples were characterized by X-ray diffraction (XRD), field-emission scanning electron microscope (FESEM), transmission electron microscope (TEM), energy dispersion spectrum (EDS), photoluminescence (PL) spectrum, Inductively coupled plasma (ICP), UV-visible (UV-vis spectroscopy), thermal gravimetric-differential thermal analysis (TG/DTA) and Fourier transform infrared (FTIR)analysis. The optimized sample synthesized with CA:G:TM mole ratio of (1.06:1.06:1) had the average particle size of 30-40 nm with a spherical morphology. Moreover, the optimized sample showed visible photoluminescence, at 400-800 nm.

AB - In this research, zirconium lanthanum and neodymium tri-doped yttria nanopowder was synthesized using the sol-gel combustion method. Citric acid (CA) and glycine (G) were used for the gel and fuel agent, respectively. The effect of CA:G:TM (TM=transition metal) mole ratios on the particle size and morphology of the product was evaluated. As-synthesized samples were characterized by X-ray diffraction (XRD), field-emission scanning electron microscope (FESEM), transmission electron microscope (TEM), energy dispersion spectrum (EDS), photoluminescence (PL) spectrum, Inductively coupled plasma (ICP), UV-visible (UV-vis spectroscopy), thermal gravimetric-differential thermal analysis (TG/DTA) and Fourier transform infrared (FTIR)analysis. The optimized sample synthesized with CA:G:TM mole ratio of (1.06:1.06:1) had the average particle size of 30-40 nm with a spherical morphology. Moreover, the optimized sample showed visible photoluminescence, at 400-800 nm.

KW - Citric acid

KW - Glycine

KW - Sol-gel combustion

KW - Zirconium lanthanum and neodymium tri-doped yttria nanopowder

UR - https://www.scopus.com/pages/publications/84977929980

U2 - 10.1016/j.ceramint.2016.03.054

DO - 10.1016/j.ceramint.2016.03.054

M3 - Article

AN - SCOPUS:84977929980

SN - 0272-8842

VL - 42

SP - 10551

EP - 10558

JO - Ceramics International

JF - Ceramics International

IS - 9

ER -