Synthesis and Characterization of Yttria Nanopowders by Precipitation Method

Mohammad Khajelakzay; Reza Shoja Razavi; Masoud Barekat

doi:10.1080/0371750X.2015.1089189

Synthesis and Characterization of Yttria Nanopowders by Precipitation Method

Mohammad Khajelakzay, Reza Shoja Razavi, Masoud Barekat

Research output: Journal Publication › Article › peer-review

7 Citations (Scopus)

Abstract

In this investigation, yttria nanopowder was synthesized by precipitation method using yttria micro powder and ammonium hydrogen carbonate as precursor materials. The most important parameters, aging time and calcination temperature, have been reviewed in detail. The effects of aging time (3, 6, 12 and 24 h) and calcination temperature (700^o, 800^o, 900^o, 1000^o and 1100^oC) were studied. Disk samples were fabricated from nanopowder at 1800^oC and 50 Mpa via SPS method. Synthesized phases, thermal behaviour and particle size were shown by X-ray diffraction pattern, thermogravimetry and differential thermal analysis, and field emission scanning electron microscopy, respectively. Fourier transform infrared spectroscopy was used for bonding study before and after heat treatment at different temperatures.

Original language	English
Pages (from-to)	208-212
Number of pages	5
Journal	Transactions of the Indian Ceramic Society
Volume	74
Issue number	4
DOIs	https://doi.org/10.1080/0371750X.2015.1089189
Publication status	Published - 2 Oct 2015
Externally published	Yes

Keywords

Aging time
Concentration
Nanopowder
Precipitation
Yttrium oxide

ASJC Scopus subject areas

Ceramics and Composites

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10.1080/0371750X.2015.1089189

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title = "Synthesis and Characterization of Yttria Nanopowders by Precipitation Method",

abstract = "In this investigation, yttria nanopowder was synthesized by precipitation method using yttria micro powder and ammonium hydrogen carbonate as precursor materials. The most important parameters, aging time and calcination temperature, have been reviewed in detail. The effects of aging time (3, 6, 12 and 24 h) and calcination temperature (700o, 800o, 900o, 1000o and 1100oC) were studied. Disk samples were fabricated from nanopowder at 1800oC and 50 Mpa via SPS method. Synthesized phases, thermal behaviour and particle size were shown by X-ray diffraction pattern, thermogravimetry and differential thermal analysis, and field emission scanning electron microscopy, respectively. Fourier transform infrared spectroscopy was used for bonding study before and after heat treatment at different temperatures.",

keywords = "Aging time, Concentration, Nanopowder, Precipitation, Yttrium oxide",

author = "Mohammad Khajelakzay and Razavi, \{Reza Shoja\} and Masoud Barekat",

note = "Publisher Copyright: {\textcopyright} 2015 Indian Ceramic Society.",

year = "2015",

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doi = "10.1080/0371750X.2015.1089189",

language = "English",

volume = "74",

pages = "208--212",

journal = "Transactions of the Indian Ceramic Society",

issn = "0371-750X",

publisher = "Taylor and Francis Ltd.",

number = "4",

}

TY - JOUR

T1 - Synthesis and Characterization of Yttria Nanopowders by Precipitation Method

AU - Khajelakzay, Mohammad

AU - Razavi, Reza Shoja

AU - Barekat, Masoud

PY - 2015/10/2

Y1 - 2015/10/2

N2 - In this investigation, yttria nanopowder was synthesized by precipitation method using yttria micro powder and ammonium hydrogen carbonate as precursor materials. The most important parameters, aging time and calcination temperature, have been reviewed in detail. The effects of aging time (3, 6, 12 and 24 h) and calcination temperature (700o, 800o, 900o, 1000o and 1100oC) were studied. Disk samples were fabricated from nanopowder at 1800oC and 50 Mpa via SPS method. Synthesized phases, thermal behaviour and particle size were shown by X-ray diffraction pattern, thermogravimetry and differential thermal analysis, and field emission scanning electron microscopy, respectively. Fourier transform infrared spectroscopy was used for bonding study before and after heat treatment at different temperatures.

AB - In this investigation, yttria nanopowder was synthesized by precipitation method using yttria micro powder and ammonium hydrogen carbonate as precursor materials. The most important parameters, aging time and calcination temperature, have been reviewed in detail. The effects of aging time (3, 6, 12 and 24 h) and calcination temperature (700o, 800o, 900o, 1000o and 1100oC) were studied. Disk samples were fabricated from nanopowder at 1800oC and 50 Mpa via SPS method. Synthesized phases, thermal behaviour and particle size were shown by X-ray diffraction pattern, thermogravimetry and differential thermal analysis, and field emission scanning electron microscopy, respectively. Fourier transform infrared spectroscopy was used for bonding study before and after heat treatment at different temperatures.

KW - Aging time

KW - Concentration

KW - Nanopowder

KW - Precipitation

KW - Yttrium oxide

UR - https://www.scopus.com/pages/publications/84954368106

U2 - 10.1080/0371750X.2015.1089189

DO - 10.1080/0371750X.2015.1089189

M3 - Article

AN - SCOPUS:84954368106

SN - 0371-750X

VL - 74

SP - 208

EP - 212

JO - Transactions of the Indian Ceramic Society

JF - Transactions of the Indian Ceramic Society

IS - 4

ER -

Synthesis and Characterization of Yttria Nanopowders by Precipitation Method

Abstract

Keywords

ASJC Scopus subject areas

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