Large-scale synthesis of YSZ nanopowder by Pechini method

Morteza Hajizadeh-Oghaz; Reza Shoja Razavi; Mohammadreza Loghman Estarki

doi:10.1007/s12034-014-0033-2

Large-scale synthesis of YSZ nanopowder by Pechini method

Morteza Hajizadeh-Oghaz, Reza Shoja Razavi, Mohammadreza Loghman Estarki

Research output: Journal Publication › Article › peer-review

26 Citations (Scopus)

Abstract

Yttria-stabilized zirconia nanopowders were synthesized on a relatively large scale using Pechini method. In the present paper, nearly spherical yttria-stabilized zirconia nanopowders with tetragonal structure were synthesized by Pechini process from zirconium oxynitrate hexahydrate, yttrium nitrate, citric acid and ethylene glycol. The phase and structural analyses were accomplished by X-ray diffraction; morphological analysis was carried out by field emission scanning electron microscopy and transmission electron microscopy. The results revealed nearly spherical yttria-stabilized zirconia powder with tetragonal crystal structure and chemical purity of 99.1% by inductively coupled plasma optical emission spectroscopy on a large scale.

Original language	English
Pages (from-to)	969-973
Number of pages	5
Journal	Bulletin of Materials Science
Volume	37
Issue number	5
DOIs	https://doi.org/10.1007/s12034-014-0033-2
Publication status	Published - Aug 2014
Externally published	Yes

Keywords

Large scale
Nanopowder
Pechini method
Sol-gel
Yttria-stabilized zirconia

ASJC Scopus subject areas

General Materials Science
Mechanics of Materials

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10.1007/s12034-014-0033-2

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title = "Large-scale synthesis of YSZ nanopowder by Pechini method",

abstract = "Yttria-stabilized zirconia nanopowders were synthesized on a relatively large scale using Pechini method. In the present paper, nearly spherical yttria-stabilized zirconia nanopowders with tetragonal structure were synthesized by Pechini process from zirconium oxynitrate hexahydrate, yttrium nitrate, citric acid and ethylene glycol. The phase and structural analyses were accomplished by X-ray diffraction; morphological analysis was carried out by field emission scanning electron microscopy and transmission electron microscopy. The results revealed nearly spherical yttria-stabilized zirconia powder with tetragonal crystal structure and chemical purity of 99.1\% by inductively coupled plasma optical emission spectroscopy on a large scale.",

keywords = "Large scale, Nanopowder, Pechini method, Sol-gel, Yttria-stabilized zirconia",

author = "Morteza Hajizadeh-Oghaz and Razavi, \{Reza Shoja\} and Estarki, \{Mohammadreza Loghman\}",

year = "2014",

month = aug,

doi = "10.1007/s12034-014-0033-2",

language = "English",

volume = "37",

pages = "969--973",

journal = "Bulletin of Materials Science",

issn = "0250-4707",

publisher = "Indian Academy of Sciences",

number = "5",

}

TY - JOUR

T1 - Large-scale synthesis of YSZ nanopowder by Pechini method

AU - Hajizadeh-Oghaz, Morteza

AU - Razavi, Reza Shoja

AU - Estarki, Mohammadreza Loghman

PY - 2014/8

Y1 - 2014/8

N2 - Yttria-stabilized zirconia nanopowders were synthesized on a relatively large scale using Pechini method. In the present paper, nearly spherical yttria-stabilized zirconia nanopowders with tetragonal structure were synthesized by Pechini process from zirconium oxynitrate hexahydrate, yttrium nitrate, citric acid and ethylene glycol. The phase and structural analyses were accomplished by X-ray diffraction; morphological analysis was carried out by field emission scanning electron microscopy and transmission electron microscopy. The results revealed nearly spherical yttria-stabilized zirconia powder with tetragonal crystal structure and chemical purity of 99.1% by inductively coupled plasma optical emission spectroscopy on a large scale.

AB - Yttria-stabilized zirconia nanopowders were synthesized on a relatively large scale using Pechini method. In the present paper, nearly spherical yttria-stabilized zirconia nanopowders with tetragonal structure were synthesized by Pechini process from zirconium oxynitrate hexahydrate, yttrium nitrate, citric acid and ethylene glycol. The phase and structural analyses were accomplished by X-ray diffraction; morphological analysis was carried out by field emission scanning electron microscopy and transmission electron microscopy. The results revealed nearly spherical yttria-stabilized zirconia powder with tetragonal crystal structure and chemical purity of 99.1% by inductively coupled plasma optical emission spectroscopy on a large scale.

KW - Large scale

KW - Nanopowder

KW - Pechini method

KW - Sol-gel

KW - Yttria-stabilized zirconia

UR - https://www.scopus.com/pages/publications/84939943152

U2 - 10.1007/s12034-014-0033-2

DO - 10.1007/s12034-014-0033-2

M3 - Article

AN - SCOPUS:84939943152

SN - 0250-4707

VL - 37

SP - 969

EP - 973

JO - Bulletin of Materials Science

JF - Bulletin of Materials Science

IS - 5

ER -

Large-scale synthesis of YSZ nanopowder by Pechini method

Abstract

Keywords

ASJC Scopus subject areas

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