Large scale synthesis of non-transformable tetragonal Sc2O 3, Y2O3 doped ZrO2 nanopowders via the citric acid based gel method to obtain plasma sprayed coating

Mohammad Reza Loghman-Estarki; Hossein Edris; Reza Shoja Razavi

doi:10.1016/j.ceramint.2013.03.042

Large scale synthesis of non-transformable tetragonal Sc₂O ₃, Y₂O₃ doped ZrO₂ nanopowders via the citric acid based gel method to obtain plasma sprayed coating

Mohammad Reza Loghman-Estarki, Hossein Edris, Reza Shoja Razavi

Research output: Journal Publication › Article › peer-review

29 Citations (Scopus)

Abstract

Non-transformable tetragonal scandia, yttria doped zirconia (SYDZ) nanopowders were prepared in large scale by the citric acid (CA) based gel method. The effect of ethylene glycol monobutyl ether (EGM):CA ratios and pH on the structure, morphology and SYDZ particle size was investigated. The microstructure of SYDZ was characterized by XRD, Raman scattering, TG-DTA, SEM, TEM, and FTIR analyses. The SYDZ nanopowders, synthesized with 1Zr ⁴⁺:4EGM:4CA mole ratio in acidic medium (pH ∼1) at 700° C, had an average diameter of 15±2 nm. Finally, air plasma spray (APS) coatings were produced from nanostructured SYDZ agglomerated powders.

Original language	English
Pages (from-to)	7817-7829
Number of pages	13
Journal	Ceramics International
Volume	39
Issue number	7
DOIs	https://doi.org/10.1016/j.ceramint.2013.03.042
Publication status	Published - Sept 2013
Externally published	Yes

Keywords

A. Sol-gel
Metastable tetragonal
Zirconia based ceramics

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Ceramics and Composites
Process Chemistry and Technology
Surfaces, Coatings and Films
Materials Chemistry

Access to Document

10.1016/j.ceramint.2013.03.042

Cite this

@article{90d039caf7c049db9c13af3d03950994,

title = "Large scale synthesis of non-transformable tetragonal Sc2O 3, Y2O3 doped ZrO2 nanopowders via the citric acid based gel method to obtain plasma sprayed coating",

abstract = "Non-transformable tetragonal scandia, yttria doped zirconia (SYDZ) nanopowders were prepared in large scale by the citric acid (CA) based gel method. The effect of ethylene glycol monobutyl ether (EGM):CA ratios and pH on the structure, morphology and SYDZ particle size was investigated. The microstructure of SYDZ was characterized by XRD, Raman scattering, TG-DTA, SEM, TEM, and FTIR analyses. The SYDZ nanopowders, synthesized with 1Zr 4+:4EGM:4CA mole ratio in acidic medium (pH ∼1) at 700° C, had an average diameter of 15±2 nm. Finally, air plasma spray (APS) coatings were produced from nanostructured SYDZ agglomerated powders.",

keywords = "A. Sol-gel, Metastable tetragonal, Zirconia based ceramics",

author = "Loghman-Estarki, \{Mohammad Reza\} and Hossein Edris and \{Shoja Razavi\}, Reza",

year = "2013",

month = sep,

doi = "10.1016/j.ceramint.2013.03.042",

language = "English",

volume = "39",

pages = "7817--7829",

journal = "Ceramics International",

issn = "0272-8842",

publisher = "Elsevier Ltd.",

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TY - JOUR

T1 - Large scale synthesis of non-transformable tetragonal Sc2O 3, Y2O3 doped ZrO2 nanopowders via the citric acid based gel method to obtain plasma sprayed coating

AU - Loghman-Estarki, Mohammad Reza

AU - Edris, Hossein

AU - Shoja Razavi, Reza

PY - 2013/9

Y1 - 2013/9

N2 - Non-transformable tetragonal scandia, yttria doped zirconia (SYDZ) nanopowders were prepared in large scale by the citric acid (CA) based gel method. The effect of ethylene glycol monobutyl ether (EGM):CA ratios and pH on the structure, morphology and SYDZ particle size was investigated. The microstructure of SYDZ was characterized by XRD, Raman scattering, TG-DTA, SEM, TEM, and FTIR analyses. The SYDZ nanopowders, synthesized with 1Zr 4+:4EGM:4CA mole ratio in acidic medium (pH ∼1) at 700° C, had an average diameter of 15±2 nm. Finally, air plasma spray (APS) coatings were produced from nanostructured SYDZ agglomerated powders.

AB - Non-transformable tetragonal scandia, yttria doped zirconia (SYDZ) nanopowders were prepared in large scale by the citric acid (CA) based gel method. The effect of ethylene glycol monobutyl ether (EGM):CA ratios and pH on the structure, morphology and SYDZ particle size was investigated. The microstructure of SYDZ was characterized by XRD, Raman scattering, TG-DTA, SEM, TEM, and FTIR analyses. The SYDZ nanopowders, synthesized with 1Zr 4+:4EGM:4CA mole ratio in acidic medium (pH ∼1) at 700° C, had an average diameter of 15±2 nm. Finally, air plasma spray (APS) coatings were produced from nanostructured SYDZ agglomerated powders.

KW - A. Sol-gel

KW - Metastable tetragonal

KW - Zirconia based ceramics

UR - https://www.scopus.com/pages/publications/84880263611

U2 - 10.1016/j.ceramint.2013.03.042

DO - 10.1016/j.ceramint.2013.03.042

M3 - Article

AN - SCOPUS:84880263611

SN - 0272-8842

VL - 39

SP - 7817

EP - 7829

JO - Ceramics International

JF - Ceramics International

IS - 7

ER -